反应条件
in tetrahydrofuran byproducts: o-tolylboronic acid; to srirred soln. of Sn-compound in THF was added soln. of BH3 in THF under N2, mixt. was left at room temp. for 1 h, refluxed for 1 h, cooled, Et2O and water was added; dried with MgSO4, solvent was removed under vac., column chromy. on silica gel with hexane and hexane-Et2O, recrystd. from water;
参考文献
Faraoni; Koll; Mandolesi; Zuniga; Podesta
Journal of Organometallic Chemistry, 2000 , vol. 613, # 2 p. 236 - 238
