2-叠氮-2-脱氧-1,3,4,6-四-氧-乙酰-Alpha-D-吡喃甘露糖合成路线 （共 8 条）
反应条件
sodium azide in N,N-dimethyl-formamide T=60°C; 0.5 h;
参考文献
Teodorovic, Peter; Slaettegard, Rikard; Oscarson, Stefan
Carbohydrate Research, 2005 , vol. 340, # 17 p. 2675 - 2676
反应条件
sulfuric acid T=20°C; 2.5 h;
参考文献
Marchesan, Silvia; Macmillan, Derek
Chemical Communications, 2008 , # 36 p. 4321 - 4323
反应条件
sulfuric acid T=0°C; 1 h;
参考文献
Krist, Pavel; Kuzma, Marek; Pelyvas, Istvan F.; Simerska, Pavla; Kren, Vladimir
Collection of Czechoslovak Chemical Communications, 2003 , vol. 68, # 4 p. 801 - 811
反应条件
in acetic acid T=100°C; 1 h;
参考文献
Saxon, Eliana; Luchansky, Sarah J.; Hang, Howard C.; Yu, Chong; Lee, Sandy C.; Bertozzi, Carolyn R.
Journal of the American Chemical Society, 2002 , vol. 124, # 50 p. 14893 - 14902
反应条件
1: 97 percent / pyridine / CH2Cl2 / 1 h / -20 °C 2: 58 percent / NaN3 / dimethylformamide / 0.5 h / 60 °C View Scheme
参考文献
Carbohydrate Research, , vol. 340, # 17 p. 2675 - 2676
反应条件
azido chloride in tetrachloromethane T=0°C; 1 h; Irradiationother halogen-azide, in other solvents under irradiation or in the dark, various time and temperature; Product distribution;
参考文献
Carbohydrate Research, , vol. 98, p. 25 - 36
反应条件
sodium azide; ammonium cerium(IV) nitrate 1.) acetonitrile, ethylacetate, -40 deg C; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 133, p. C1 - C4
反应条件
sodium azide; ammonium cerium(IV) nitrate 1.) EtOAc, CH3CN, -40 deg C, 6 d; 2.) glacial acetic acid, 100 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Carbohydrate Research, , vol. 136, p. 153 - 176
