6-(甲基硫代)苯并[d][1,3]二氧代-5-胺合成路线 （共 2 条）
反应条件
1: With hydrogenchloride; ethanol; water; iron
T=110°C; 2 h;
2: in ethanol; water
pH=11; Alkaline aqueous solution;
参考文献
Cai, Xiong; Qian, Changgeng; Zhai, Haixiao
Patent: US2008/234314 A1, 2008 ;
Location in patent: Page/Page column 54 ;
US 20080234314 A1
反应条件
1: K2CO3 / ethanol / 24 h / Ambient temperature
2: Sn, conc. HCl / acetic acid / 1.5 h / 100 - 105 °C
View Scheme
参考文献
Dillard; Yen; Stark; Pavey
Journal of Medicinal Chemistry, 1980 , vol. 23, # 7 p. 717 - 722
