反应条件
1: 9,9-dimethyl-9H-xanthene With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in diethyl ether; hexane T=-40 - 20°C; 2: bis(diethylamino)phosphorochloridite in diethyl ether; hexane; pentane T=-60 - 20°C; Further stages.;
参考文献
Van Der Vlugt, Jarl Ivar; Hewat, Alison C.; Neto, Samuel; Sablong, Rafael; Mills, Allison M.; Lutz, Martin; Spek, Anthony L.; Mueller, Christian; Vogt, Dieter
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 8 p. 993 - 1003
