1,1,1,4,4,4-六氟-2,3-丁二酮合成路线 (共 16 条)
反应条件
chromium(VI) oxide; sulfuric acid; sulfur trioxide
参考文献
Ramirez,F. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 2429 - 2433
反应条件
in methanol; sodium methylate
参考文献
Icagen, Inc.
Patent: US2003/176450 A1, 2003 ;
参考文献
Krespan,C.G. et al.
Journal of the American Chemical Society, 1977 , vol. 99, p. 1214 - 1217
反应条件
sulfuric acid
T=70°C; 2 h;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Russian Journal of Nondestructive Testing, 1997 , vol. 33, # 2 p. 265 - 272
反应条件
T=500°C; P=0.4 Torr;
参考文献
Coe, Paul L.; Cook, Michael I.; Owen, Ian R.
Journal of Fluorine Chemistry, 1989 , vol. 42, p. 389 - 402
反应条件
potassium permanganate in water; acetone
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Knunyants, I. L.; Postovoi, S. A.; Delyagina, N. I.; Zeifman, Yu. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 10 p. 2090 - 2095
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 10 p. 2256 - 2261
反应条件
T=440°C; P=0.4 Torr;
参考文献
Coe, Paul L.; Cook, Michael I.; Owen, Ian R.
Journal of Fluorine Chemistry, 1989 , vol. 42, p. 389 - 402
反应条件
in diethylene glycol dimethyl ether
1 h; Ambient temperature; Further byproducts given;
参考文献
Saloutina; Zapevalov; Kodess; Saloutin
Journal of Fluorine Chemistry, 1998 , vol. 87, # 1 p. 49 - 55
反应条件
ozone
T=-262.16°C; Ar-matrix; Product distribution; Further Variations:Solvents;
参考文献
Singmaster; Jonnalagadda; Chan
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9078 - 9088
反应条件
pentacarbonyliron(0)
参考文献
Filatov,A.S.; Englin,M.A.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 11 p. 2316 - 2319,2407 - 2409