3-氯-N,N-二甲基苯胺合成路线 (共 30 条)
反应条件
methanol; hydrogen T=99.84°C; P=9750.98 Torr; 1.25 h; Autoclave;
参考文献
Catalysis Communications, , vol. 41, p. 115 - 118
反应条件
Zr(BH4)2Cl2(dabco)2; zirconium tetrachloride in methanol; water T=20°C; 0.7 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Alinezhad, Heshmatollah
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 1 p. 143 - 151
反应条件
potassium nitrate in dimethyl sulfoxide T=25°C; 0.0333333 h; Rate constant;
参考文献
Bordwell, Frederick G.; Hughes, David L.
Journal of the American Chemical Society, 1986 , vol. 108, # 23 p. 7300 - 7309
反应条件
sulfuric acid T=200°C; 16 h;
参考文献
Kato, Taka-aki; Matsuda, Tomonari; Matsui, Saburo; Mizutani, Takaharu; Saeki, Ken-ichi
Biological and pharmaceutical bulletin, 2002 , vol. 25, # 4 p. 466 - 471
反应条件
formic acid; iron(II) chloride heptahydrate; triethylamine T=150°C; 12 h;
参考文献
Jiang, Xue; Wang, Chao; Wei, Yawen; Xue, Dong; Liu, Zhaotie; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 58 - 63
反应条件
methanesulfonic acid; hydrogen; [Ru(acac)3]; 1,1,1-tris (diphenylphosphinomethyl)ethane in tetrahydrofuran T=140°C; 36 h; AutoclaveInert atmosphere;
参考文献
Li, Yuehui; Sorribes, Ivan; Yan, Tao; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2013 , vol. 52, # 46 p. 12156 - 12160
Angew. Chem., 2013 , vol. 125, # 46 p. 12378 - 12382,5
反应条件
C27H36Cl2N2Zn; phenyl silane in tetrahydrofuran T=100°C; 20 h;
参考文献
Chemical Science, , vol. 4, # 5 p. 2127 - 2131
参考文献
Journal of the American Chemical Society, , vol. 68, p. 895
参考文献
Journal of the Chemical Society, , p. 1145
参考文献
Chemische Berichte, , vol. 16, p. 32