4-甲基-1-苯基戊烷-3-醇合成路线 （共 13 条）
反应条件
sodium t-butanolate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in toluene
T=110°C; 17 h;
参考文献
Fujita, Ken-Ichi; Asai, Chiho; Yamaguchi, Tetsuhiro; Hanasaka, Fumihiro; Yamaguchi, Ryohei
Organic Letters, 2005 , vol. 7, # 18 p. 4017 - 4019
反应条件
1: With 1-bromo-butane; RhCl(PPh3)3 in toluene
T=55°C;
2: With boron trifluoride diethyl etherate in toluene
T=55°C;
参考文献
Shi, Lei; Tu, Yong-Qiang; Wang, Min; Zhang, Fu-Min; Fan, Chun-An; Zhao, Yu-Ming; Xia, Wu-Jiong
Journal of the American Chemical Society, 2005 , vol. 127, # 31 p. 10836 - 10837
反应条件
indium; copper(l) iodide; iodine in water
T=20°C; Barbier reaction; 48 h;
参考文献
Shen, Zhi-Liang; Yeo, Yan-Lin; Loh, Teck-Peng
Journal of Organic Chemistry, 2008 , vol. 73, # 10 p. 3922 - 3924
反应条件
lithium borohydride in tetrahydrofuran
T=-20°C; 24 h;
参考文献
Comins, Daniel L.; Herrick, James J.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1321 - 1324
反应条件
(i) Mg, Et2O, (ii) /BRN= 605330/; Multistep reaction;
参考文献
Julia,M.; Labia,R.
Bulletin de la Societe Chimique de France, 1972 , p. 4151 - 4157
反应条件
sodium tetrahydroborate; (2,2'-bipyridine-N,N')dichloronickel in methanol
参考文献
Handique, Jyotirekha G.; Purkayashtha, Arup; Baruah, Jubaraj B.
Journal of Organometallic Chemistry, 2001 , vol. 620, # 1-2 p. 90 - 93
反应条件
dibenzoyl peroxide in acetonitrile
T=80°C; 48 h;
参考文献
Julia,M.; Mansuy,D.
Bulletin de la Societe Chimique de France, 1972 , p. 2684 - 2689
参考文献
Bogert; Davidson; Apfelbaum
Journal of the American Chemical Society, 1934 , vol. 56, p. 959,961
反应条件
scandium tris(trifluoromethanesulfonate) in dichloromethane-d2
T=-78°C; Kinetics; Further Variations:Temperatures;
参考文献
Rauniyar, Vivek; Hall, Dennis G.
Journal of the American Chemical Society, 2004 , vol. 126, # 14 p. 4518 - 4519
反应条件
sodium tetrahydroborate
参考文献
Li, Xuefeng; Li, Liangchun; Tang, Yuanfu; Zhong, Ling; Cun, Linfeng; Zhu, Jin; Liao, Jian; Deng, Jingen
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2981 - 2988
