1-环己基-2-吡咯烷酮合成路线 （共 10 条）
反应条件
[Rh2(trifluoroacetate)4]; water in toluene 10 h; RefluxInert atmosphere; chemoselective reaction;
参考文献
Oh, Yun Taek; Senda, Kousuke; Hata, Takeshi; Urabe, Hirokazu
Tetrahedron Letters, 2011 , vol. 52, # 19 p. 2458 - 2461
反应条件
hydrogen; palladium on activated carbon in 1,4-dioxane T=150°C; P=41404.1 Torr; 4 h; Product distribution / selectivity;
参考文献
US2004/192937 A1, ;
Page 6 ;
反应条件
di-tert-butyl peroxide; [Cl2NN]Cu T=20°C; 16 h;
参考文献
Georgetown University
Patent: US2011/213146 A1, 2011 ;
Location in patent: Page/Page column 3; 27 ;
反应条件
sodium tetrahydroborate; RhH(CO)(triphenylphosphine)3 in dichloromethane; isopropyl alcohol T=100°C; P=26220 Torr; 24 h;
参考文献
Zhou, Jian-Qiang; Alper, Howard
Journal of Organic Chemistry, 1992 , vol. 57, # 12 p. 3328 - 3331
反应条件
carbon tetrabromide; triphenylphosphine in acetonitrile T=60°C; 10 h;
参考文献
Yang, Yong-Hua; Shi, Min
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8645 - 8648
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=220°C; 0.583333 h; Microwave irradiation;
参考文献
Orrling, Kristina M.; Wu, Xiongyu; Russo, Francesco; Larhed, Mats
Journal of Organic Chemistry, 2008 , vol. 73, # 21 p. 8627 - 8630
反应条件
1: With copper(l) iodide; lithium tert-butylate in acetonitrile T=20°C; 0.0833333 h; Inert atmosphere; 2: in acetonitrile T=20°C; 24 h; Inert atmosphereIrradiation;
参考文献
Do, Hien-Quang; Bachman, Shoshana; Bissember, Alex C.; Peters, Jonas C.; Fu, Gregory C.
Journal of the American Chemical Society, 2014 , vol. 136, # 5 p. 2162 - 2167
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 1.2: -78 - 20 °C / Inert atmosphere 2.1: [Rh2(trifluoroacetate)4]; water / toluene / 10 h / Reflux; Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 52, # 19 p. 2458 - 2461
反应条件
p-nitrobenzenesulfonyl peroxide 1.) -78 deg C, dichloromethane, 2.) 25 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 30, # 32 p. 4207 - 4210
反应条件
9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran
T=65°C; 1 h;
参考文献
Collins, Christopher J.; Lanz, Marc; Singaram, Bakthan
Tetrahedron Letters, 1999 , vol. 40, # 19 p. 3673 - 3676
