4-氯苯 N-苯甲酰苯胺合成路线 （共 81 条）
反应条件
in methanol T=20°C; Kinetics; TemperatureConcentration; regioselective reaction;
参考文献
International Journal of Chemical Kinetics, , vol. 45, # 9 p. 551 - 559
反应条件
T=40 - 45°C; Behandeln des Reaktionsprodukts mit Wasser;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 563, p. 99,103
反应条件
T=40 - 45°C; Behandeln des Reaktionsprodukts mit Wasser;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 563, p. 99,103
反应条件
trichlorophosphate Eintragen des Reaktionsproduktes in verd. Salzsaeure;
参考文献
Hoechster Farbw.
Patent: DE290065 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 211
反应条件
1: NOCl, Py 2: CCl4 View Scheme
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1296 - 1304
反应条件
1: 61.2 percent / n-BuLi, 2-bromobenzyl bromide / tetrahydrofuran / 1.) -78 deg C, 0.5 h; r.t., 1 h, 2.) -78 deg C, 1 h; r.t., 1 h 2: 85.2 percent / conc. H2SO4 / aq. acetic acid / 3 h / Heating View Scheme
参考文献
Epsztajn, J.; Bieniek, A.; Kowalska, J. A.
Monatshefte fuer Chemie, 1996 , vol. 127, # 6/7 p. 701 - 716
反应条件
1: 1.) LDA / 1.) THF, hexane, 0 deg C, 2.) room temperature 2: 1 N sodium ethoxide / ethanol; tetrahydrofuran / Ambient temperature View Scheme
参考文献
Ono; Araya; Todoriki; Tamura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 7 p. 1824 - 1831
反应条件
1: phosphothion 2: Rb2CO3; tris-(dibenzylideneacetone)dipalladium(0); oxygen; tris-(o-tolyl)phosphine / water / 24 h / 40 °C / 760.05 Torr View Scheme
参考文献
Inamoto, Kiyofumi; Nozawa, Kanako; Kondo, Yoshinori
Synlett, 2012 , vol. 23, # 11 p. 1678 - 1682
反应条件
Bi(NO3)3·5H2O; acetic anhydride in dichloromethane T=23°C; regioselective reaction;
参考文献
Lu, Yang; Li, Yaming; Zhang, Rong; Jin, Kun; Duan, Chunying
Tetrahedron, 2013 , vol. 69, # 45 p. 9422 - 9427
反应条件
1: 47 percent / n-BuLi / tetrahydrofuran / 1.) -78 deg C, 0.5 h; r.t., 1 h, 2.) -78 deg C, 1 h; r.t., 1 h 2: 72.9 percent / conc. H2SO4 / aq. acetic acid / 24 h / Heating 3: conc. H2SO4 / 5 h 4: aq. K2Cr2O7 / aq. acetic acid / 1 h / 90 °C View Scheme
参考文献
Epsztajn, J.; Bieniek, A.; Kowalska, J. A.
Monatshefte fuer Chemie, 1996 , vol. 127, # 6/7 p. 701 - 716
