3,6-二苯基-1,2,4,5-四嗪合成路线 (共 59 条)
反应条件
in tetrahydrofuran 2 h; -70 deg C -> room temperature; analogous reaction with lithium diethylamide, pathway including two competing reactions is proposed; Product distribution;
参考文献
Hunter, Daniel; Neilson, Douglas G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1601 - 1603
反应条件
in tetrahydrofuran 2 h; -70 deg C -> room temperature; analogous reaction with lithium diethylamide, pathway including two competing reactions is proposed; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1601 - 1603
反应条件
potassium hydroxide in methanol Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1081 - 1086
反应条件
potassium hydroxide in methanol 240 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1081 - 1086
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 102, p. 132
反应条件
in toluene 40 h; Heating;
参考文献
Figeys, H. P.; Mathy, A.
Tetrahedron Letters, 1981 , vol. 22, # 15 p. 1393 - 1396
反应条件
sodium tetrahydroborate
参考文献
Hu, Wei-Xiao; Xu, Feng
Journal of Chemical Research, 2006 , # 12 p. 797 - 799
反应条件
in diethyl ether; dichloromethane
参考文献
Neugebauer, Franz Alfred; Krieger, Claus; Fischer, Hans; Siegel, Rolf
Chemische Berichte, 1983 , vol. 116, # 6 p. 2261 - 2274
反应条件
in ethanol soln. Ru complex and 1,2,4,5-tetrazine ligand in EtOH was heated to reflux for 5 h under aerobic conditions; soln. was evapd. to dryness in vacuo, residue was dissolved in CH2Cl2 and chromed. on silica column (CH2Cl2-MeCN) followed by prep. TLC on silica; elem. anal.;
参考文献
Inorganic Chemistry, , vol. 45, # 3 p. 1316 - 1325
反应条件
in tetrahydrofuran
Inverse Electron Demand Diels-Alder (IED-DA) reaction; 0.333333 h;
参考文献
University of Delaware
Patent: US2009/23916 A1, 2009 ;
Location in patent: Page/Page column 20 ;