1: 6.9 g / hydrogen / 10percent Pd-C / acetic acid / Ambient temperature; Parr apparatus 2: 93 percent / thionyl chloride / 1.) 50 deg C, 4 h, 2.) room temperature, 48 h 3: 82.4 percent / 1 M NaHCO3 / ethyl acetate 4: 50 mg / 1 M HCl / ethanol / 48 h / Heating View Scheme

4-(N,N-dimethlyamino)pyridine; triethylamine in tetrahydrofuran

1: 82.4 percent / 1 M NaHCO3 / ethyl acetate 2: 50 mg / 1 M HCl / ethanol / 48 h / Heating View Scheme

1: 82.4 percent / 1 M NaHCO3 / ethyl acetate 2: 50 mg / 1 M HCl / ethanol / 48 h / Heating View Scheme

1: 93 percent / thionyl chloride / 1.) 50 deg C, 4 h, 2.) room temperature, 48 h 2: 82.4 percent / 1 M NaHCO3 / ethyl acetate 3: 50 mg / 1 M HCl / ethanol / 48 h / Heating View Scheme

hydrogenchloride in ethanol 48 h; Heating;

暂无反应条件数据

1: N2H4*H2O / ethanol / Heating 2: Br2, AcOH / 40 °C View Scheme