3-(2-吡啶基二硫基)丙酸N-羟基琥珀酰亚胺酯合成路线 （共 6 条）
反应条件
dicyclohexyl-carbodiimide in tetrahydrofuran 0 deg C, 1 h, then 20 deg C, 2 h;
参考文献
Shval'e, A. F.; Ofitserov, V. I.; Samukov, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 9 p. 2152,1909 - 1910
反应条件
1,4-diaza-bicyclo[2.2.2]octane; dicyclohexyl-carbodiimide in dichloromethane T=0°C; -40 deg C to -5 deg C, 0 deg C, overnight;
参考文献
Loccufier, J.; Schacht, E.
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 7 p. 535 - 540
反应条件
1: 77 percent / AcOH / ethanol / 2 h / 20 °C 2: 79 percent / dicyclohexylcarbodiimide / CH2Cl2 / 3 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 31 p. 9640 - 9649
反应条件
boron trifluoride-diethyl ether complex in ethyl acetate
反应条件
1: acetic acid / 1 h / 20 °C 2: 80 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 0 deg C, 1 h, then 20 deg C, 2 h View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 9 p. 2152,1909 - 1910
反应条件
1: 37 percent aq. HCl / dioxane / 60 °C 2: 75 percent / 1,4-diazabicyclo<2.2.2>octane, dicyclohexyl carbodiimide / CH2Cl2 / 0 °C / -40 deg C to -5 deg C, 0 deg C, overnight View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 97, # 7 p. 535 - 540
