2-甲基-1,4,7,10,13-五氧杂环十五烷合成路线 （共 3 条）
反应条件
sodium methylate
1.) sodium methoxide, dioxane, diol, 10 min 2.) 1,2-bis<2'-(toluene-p-sulphonyloxy)ethoxy>ethane, dioxane, 5 min, reflux; Multistep reaction;
参考文献
Bowsher, Brian R.; Rest, Antony J.; Main, Brian G.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1421 - 1426
反应条件
Yield given. Multistep reaction;
参考文献
Ikeda, Isao; Yamamura, Shingo; Nakatsuji, Yohji; Okahara, Mitsuo
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5355 - 5358
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=50°C; 12 h;
参考文献
Li, Cong; Wong, Wing-Tak
Chemical Communications, 2002 , # 18 p. 2034 - 2035
