反应条件
1: 86 percent / 10percent Pd/C / 2 h / 300 - 320 °C
2: 78 percent / Br2 / chlorobenzene / 0.25 h / Ambient temperature
3: 91 percent / Cl2 / various solvent(s) / 0.33 h / Ambient temperature
4: 95 percent / n-Butyllithium/hexane / diethyl ether / 0.5 h / Heating
5: hexamethylphosphoric acid triamide / 20 h / 100 °C
6: 66 percent / n-Butyllithium / diethyl ether / 0.5 h / Heating
7: 99 percent / Ethanethiol, NaH / dimethylformamide / 3 h / Heating
View Scheme
参考文献
Lee; Shyamasundar; Harvey
Journal of Organic Chemistry, 1981 , vol. 46, # 14 p. 2889 - 2895