2-羟基-3-甲氧基苯甲腈合成路线 （共 12 条）
反应条件
anhydrous iron chloride; hydroxylamine hydrochloride in N,N-dimethyl-formamide 3 h; Reflux;
参考文献
Ghosh, Pranab; Subba, Raju
Tetrahedron Letters, 2013 , vol. 54, # 36 p. 4885 - 4887
反应条件
thionyl chloride in diethyl ether Heating;
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
und Behandeln des Reaktionsprodukts mit wss.KOH unterhalb 40grad;
参考文献
Journal of the Chemical Society, , p. 1651
反应条件
potassium carbonate in acetone Yield given;
参考文献
Wollenweber, Eckhard; Mann, Karin; Iinuma, Munekazu; Tanaka, Toshiyuki; Mizuno, Mizuo
Phytochemistry (Elsevier), 1988 , vol. 27, # 5 p. 1483 - 1486
反应条件
hydrogenchloride; sodium chloride; iodine; magnesium in water; methoxybenzene; toluene
参考文献
Fahrig, Thomas; Gerlach, Irene; Horvath, Ervin; Jork, Reinhard; Mauler, Frank
Patent: US2002/177616 A1, 2002 ;
反应条件
1: K2CO3 / acetone 2: Mg / diethyl ether / 15 h / Heating View Scheme
参考文献
Wollenweber, Eckhard; Mann, Karin; Iinuma, Munekazu; Tanaka, Toshiyuki; Mizuno, Mizuo
Phytochemistry (Elsevier), 1988 , vol. 27, # 5 p. 1483 - 1486
反应条件
diethyl ether und Erwaermen des Reaktionsprodukts mit wss.HCl;
参考文献
Borsche; Hahn-Weinheimer
Justus Liebigs Annalen der Chemie, 1959 , vol. 570, p. 155,163
反应条件
1: K2CO3 / acetone 2: Mg / diethyl ether / 15 h / Heating 3: 5N KOH / 2-methoxy-ethanol 4: DDQ / dioxane / 7 h / Heating View Scheme
参考文献
Wollenweber, Eckhard; Mann, Karin; Iinuma, Munekazu; Tanaka, Toshiyuki; Mizuno, Mizuo
Phytochemistry (Elsevier), 1988 , vol. 27, # 5 p. 1483 - 1486
反应条件
potassium hydroxide in tetrahydrofuran; water
Ambient temperature;
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
反应条件
1: 92 percent / KOH / tetrahydrofuran; H2O / Ambient temperature
2: 95 percent / diphenyl ether / 0.5 h / 240 - 250 °C
View Scheme
参考文献
Rahman, Loay K. A.; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 12 p. 2973 - 2978
