1-环己基-2,5-二氢-1H-吡咯合成路线 （共 4 条）
反应条件
Grubb's 2nd generation catalyst in dichloromethane
T=50°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Sawadjoon, Supaporn; Samec, Joseph S. M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2548 - 2554
反应条件
copper(l) iodide; diisopropylamine in 1,4-dioxane
Cyclization; 3 h; Heating;
参考文献
Jayaprakash, Karamil; Venkatachalam, Chittoor S.; Balasubramanian, Kalpattu K.
Tetrahedron Letters, 1999 , vol. 40, # 35 p. 6493 - 6496
反应条件
in dichloromethane
Ambient temperature;
参考文献
Ding, Zhaozhong; Tufariello, Joseph J.
Synthetic Communications, 1990 , vol. 20, # 2 p. 227 - 230
反应条件
1: triethyl borane; tributylphosphine; palladium diacetate / tetrahydrofuran / 19 h / 66 °C / Inert atmosphere
2: Grubb's 2nd generation catalyst / dichloromethane / 1 h / 50 °C / Inert atmosphere; Microwave irradiation
View Scheme
参考文献
Sawadjoon, Supaporn; Samec, Joseph S. M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2548 - 2554
