2,4-二硝基-苯乙酸乙酯合成路线 （共 38 条）
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether
T=-20 - 0°C;
参考文献
Haglund; Nilsson
Synthesis, 1994 , # 3 p. 242 - 243
反应条件
hydrogenchloride in diethyl ether
T=20°C;
参考文献
Prueger, Birgit; Hofmeister, Gretchen E.; Jacobsen, Christian Borch; Alberg, David G.; Nielsen, Martin; Jorgensen, Karl Anker
Chemistry - A European Journal, 2010 , vol. 16, # 12 p. 3783 - 3790
反应条件
tetrabutyl ammonium fluoride
4 h; Ambient temperatureIrradiation;
参考文献
Cervera, Maria; Marquet, Jordi
Tetrahedron Letters, 1996 , vol. 37, # 42 p. 7591 - 7594
反应条件
copper(I) bromide in tetrachloromethane
参考文献
Kovalenko, S. V.; Artamkina, G. A.; Beletskaya, I. P.; Reutov, O. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 12 p. 2668
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 12 p. 2869 - 2870
反应条件
1: concentrated sulfuric acid; fuming nitric acid
View Scheme
参考文献
Gabriel; Meyer
Chemische Berichte, 1881 , vol. 14, p. 830
反应条件
in benzene-d6
T=30°C; 4 h; Kinetics; SolventConcentration;
参考文献
Hirai, Sho; Asahara, Haruyasu; Hirao, Shotaro; Sawayama, Jun; Sugimoto, Ryuichi; Saigo, Kazuhiko; Nishiwaki, Nagatoshi
RSC Advances, 2014 , vol. 4, # 10 p. 4889 - 4892
反应条件
1: nickel; ethanol; ethyl acetate / Hydrogenation.weiteres Reagens: Wasser
2: ethanol; ethyl acetate; aqueous HCl
3: pyridine
View Scheme
参考文献
Ruggli; Grand
Helvetica Chimica Acta, 1937 , vol. 20, p. 373,383
反应条件
sodium ethanolate; isopentyl nitrite in ethanol
T=60°C; 1 h;
参考文献
Schumacher, Richard; Danca, Mihaela Diana; Ma, Jianguo; Herbert, Brian; Nguyen, True Minh; Xie, Wenge; Tehim, Ashok
Patent: US2007/78147 A1, 2007 ;
Location in patent: Page/Page column 73 ;
