(2,2,2-三氟-1-羟基乙基)氨基甲酸苄酯合成路线 (共 6 条)
反应条件
triethylamine in 1,4-dioxane T=20°C; 1.5 h;
参考文献
De Medina; Ingrassia; Mulliez
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8424 - 8430
反应条件
5A molecular sieve; triethylamine in dichloromethane
T=20°C; 336 h;
参考文献
Titanyuk; Vorob'eva; Osipov; Beletskaya
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 5 p. 619 - 623
反应条件
5A molecular sieve in 1,4-dioxane
Substitution; 336 h;
参考文献
Ingrassia, Laurent; Mulliez, Michel
Synthesis, 1999 , # 10 p. 1731 - 1738
反应条件
water in 1,4-dioxane
参考文献
Weygand,F. et al.
Chemische Berichte, 1966 , vol. 99, p. 1932 - 1943
反应条件
in diethylene glycol dimethyl ether
参考文献
Weygand,F. et al.
Chemische Berichte, 1966 , vol. 99, p. 1944 - 1956
反应条件
phosphorus pentachloride
参考文献
Weygand,F. et al.
Chemische Berichte, 1966 , vol. 99, p. 1944 - 1956