1-(1-环己烯-1-基磺酰基)-4-甲基苯合成路线 （共 32 条）
反应条件
1: (reduction)
2: Py
3: piperidine, piperidine*HCl / dimethylformamide / 30 °C
View Scheme
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
反应条件
1: Py
2: piperidine, piperidine*HCl / dimethylformamide / 30 °C
View Scheme
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
反应条件
2: aq. H2O2
3: (reduction)
4: Py
5: piperidine, piperidine*HCl / dimethylformamide / 30 °C
View Scheme
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
反应条件
2: aq. H2O2
3: (reduction)
4: Py
5: piperidine, piperidine*HCl / dimethylformamide / 30 °C
View Scheme
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
反应条件
piperidine; tetrahydropyridine hydrochloride in N,N-dimethyl-formamide
T=30°C; Rate constant;
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
反应条件
1: 90 percent / ethanol / 2 h / 0 °C
2: 80 percent / CCl4 / Irradiation
3: 1) 30percent H2O2, 2) NEt3 / 1) THF, -20 deg C, 2 h, 2) RT, 12 h
View Scheme
参考文献
Gancarz, Roman A.; Kice, John L.
Journal of Organic Chemistry, 1981 , vol. 46, p. 4899 - 4906
反应条件
1: 90 percent / ethanol / 2 h / 0 °C
2: 80 percent / CCl4 / Irradiation
3: 1) 30percent H2O2, 2) NEt3 / 1) THF, -20 deg C, 2 h, 2) RT, 12 h
View Scheme
参考文献
Gancarz, Roman A.; Kice, John L.
Journal of Organic Chemistry, 1981 , vol. 46, p. 4899 - 4906
反应条件
1: Na2CO3 / acetonitrile
2: 80 percent / CCl4 / Irradiation
3: 1) 30percent H2O2, 2) NEt3 / 1) THF, -20 deg C, 2 h, 2) RT, 12 h
View Scheme
参考文献
Gancarz, Roman A.; Kice, John L.
Journal of Organic Chemistry, 1981 , vol. 46, p. 4899 - 4906
反应条件
1: 68 percent / CuCl2, triethylaminium halide / acetonitrile / 40 °C
2: 76 percent / triethylamine / benzene / 48 h / Ambient temperature
View Scheme
参考文献
Liu, Lilian Kao; Chi, Y.; Jen, Kwan-Yue
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 406 - 410
反应条件
1: I2 / ethanol; H2O
2: 68 percent / CuCl2, triethylaminium halide / acetonitrile / 40 °C
3: 76 percent / triethylamine / benzene / 48 h / Ambient temperature
View Scheme
参考文献
Liu, Lilian Kao; Chi, Y.; Jen, Kwan-Yue
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 406 - 410
