2-羟基-5-(甲基硫代)苯甲醛合成路线 (共 3 条)
反应条件
triethylamine; magnesium chloride in anhydrous propionitrile
T=100°C; 5 h; Inert atmosphere;
参考文献
Hirano, Keiichi; Biju, Akkattu T.; Piel, Isabel; Glorius, Frank
Journal of the American Chemical Society, 2009 , vol. 131, # 40 p. 14190 - 14191
反应条件
paraformaldehyde in hydrogenchloride; diethyl ether; toluene
参考文献
McKearn, John P.; Gordon, Gary B.; Cunningham, James; Gately, Stephen T.; Koki, Alane T.; Masferrer, Jaime L.
Patent: US2002/103141 A1, 2002 ;
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; paraformaldehyde in diethyl ether; toluene
参考文献
G.D. Searle and Co.
Patent: US6077850 A1, 2000 ;