N-(2,4,6-三甲基苯基)甲酰胺合成路线 （共 10 条）
反应条件
lithium aluminium tetrahydride
参考文献
Dallacker,F.; Eschelbach,F.-E.
Justus Liebigs Annalen der Chemie, 1965 , vol. 689, p. 171 - 178
反应条件
choline chloride*2SnCl2
T=70°C;
参考文献
Azizi, Najmadin; Gholibeglo, Elham; Babapour, Mahbobe; Ghafuri, Hossein; Bolourtchian, Seyed Mohammad
Comptes Rendus Chimie, 2012 , vol. 15, # 9 p. 768 - 773
反应条件
choline chloride*2SnCl2 in water
T=70°C;
参考文献
Azizi, Najmadin; Gholibeglo, Elham; Babapour, Mahbobe; Ghafuri, Hossein; Bolourtchian, Seyed Mohammad
Comptes Rendus Chimie, 2012 , vol. 15, # 9 p. 768 - 773
反应条件
T=200°C; 12 h; Autoclave;
参考文献
BASF SE; BASF (CHINA) COMPANY LIMITED; HASHMI, A., Stephen K.; LOTHSCHUeTZ, Christian
Patent: WO2012/56419 A1, 2012 ;
Location in patent: Page/Page column 63 ;
反应条件
phenyl silane; C{N(2,6-iPr2C6H3)CH}2 in tetrahydrofuran
T=20°C; P=750.075 Torr; 24 h; Inert atmosphere;
参考文献
Jacquet, Olivier; Das Neves Gomes, Christophe; Ephritikhine, Michel; Cantat, Thibault
Journal of the American Chemical Society, 2012 , vol. 134, # 6 p. 2934 - 2937
反应条件
hydrogenchloride
T=250°C; P=2206520 Torr;
参考文献
Buckley; Ray
Journal of the Chemical Society, 1949 , p. 1154
反应条件
T=250°C; P=2206520 Torr;
参考文献
Buckley; Ray
Journal of the Chemical Society, 1949 , p. 1154
参考文献
Hantzsch; Lucas
Chemische Berichte, 1895 , vol. 28, p. 746
反应条件
1: With trichlorophosphate in dichloromethane
T=-60°C; 0.416667 h;
2: With triethylamine in dichloromethane
T=-60 - 20°C;
参考文献
BASF SE; BASF (CHINA) COMPANY LIMITED; HASHMI, A., Stephen K.; LOTHSCHUeTZ, Christian
Patent: WO2012/56419 A1, 2012 ;
Location in patent: Page/Page column 63 ;
反应条件
potassium tert-butylate
T=350°C;
参考文献
Marion; Oldfield
Canadian Journal of Research, Section B: Chemical Sciences, 1947 , vol. 25, p. 1,12
