反式-BETA-苯乙烯硼酸合成路线 (共 109 条)
反应条件
tetrakis(triphenylphosphine) palladium(0) in methanol T=25°C; P=760 Torr; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 344, p. C5 - C7
反应条件
carbon monoxide; tetrakis(triphenylphosphine) palladium(0) in methanol treatment with CO (1 atm) in methanol (25 ° C, 20 h, catalyst: Pd(PPh3)4); GLC;
参考文献
Journal of Organometallic Chemistry, , vol. 344, p. C5 - C7
反应条件
copper(I) thiophene-2-carboxylate in N,N-dimethyl-formamide T=50°C; 3 h;
参考文献
Organic Letters, , vol. 9, # 10 p. 1947 - 1950
反应条件
copper(I) thiophene-2-carboxylate in N,N-dimethyl-formamide T=50°C; 3 h;
参考文献
Organic Letters, , vol. 9, # 10 p. 1947 - 1950
反应条件
palladium diacetate; sodium acetate in acetic acid T=50°C; 20 h;
参考文献
Cho, Chan Sik; Uemura, Sakae
Journal of Organometallic Chemistry, 1994 , vol. 465, # 1-2 p. 85 - 92
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 4 h; Heating; Title compound not separated from byproducts;
参考文献
Ma, Shengming; Zhang, Aibin
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2287 - 2294
反应条件
palladium diacetate; sodium acetate; ethyl acrylate in acetic acid T=25°C; 20 h;
参考文献
Journal of Organometallic Chemistry, , vol. 465, # 1-2 p. 85 - 92
反应条件
1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane / 1,4-dioxane; water / 65 °C / |Inert atmosphere 2: bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran / 5 h / 25 °C / |Inert atmosphere View Scheme
参考文献
Chelucci, Giorgio
Chemical Communications, 2014 , vol. 50, # 31 p. 4069 - 4072
反应条件
palladium diacetate; sodium carbonate; (Z)-(i-Pr)CBr=C(CO2Me)NHAc in ethanol T=50 - 55°C; 2 h;
参考文献
Burk, Mark J.; Allen, John G.; Kiesman, William F.; Stoffan, Karen M.
Tetrahedron Letters, 1997 , vol. 38, # 8 p. 1309 - 1312
反应条件
[14C]-Orotic acid; caesium carbonate in acetone T=80°C; Suzuki coupling; 30 h; Inert atmosphere;
参考文献
Zhang, Hong-Ping; Dai, You-Zhi; Zhou, Xi; Yu, Huang
Synlett, 2012 , vol. 23, # 8 p. 1221 - 1224