1-(二甲氧基甲基)-4-(1-甲基乙基)-苯合成路线 （共 11 条）
反应条件
thionyl chloride; acetyl chloride T=50 - 60°C; 0.75 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Weidner, Reinhold; Wuerthwein, Ernst-Ulrich
Chemische Berichte, 1989 , vol. 122, p. 1095 - 1106
反应条件
acetate buffer; sodium lauryl sulfate in water T=25°C; pH=5.04 - 5.27; Kinetics; Further Variations:ReagentspH-values;
参考文献
Rose, Phillip D. R.; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 9 p. 1589 - 1595
参考文献
BASF Aktiengesellschaft
Patent: US4814510 A1, 1989 ;
参考文献
BASF Aktiengesellschaft
Patent: US4814510 A1, 1989 ;
反应条件
methyl methyltributylammonium sulfate
T=57°C; Electrochemical reaction;
参考文献
BASF SE
Patent: US2011/207968 A1, 2011 ;
Location in patent: Page/Page column 8-9 ;
反应条件
sodium methylate
T=25 - 30°C; 1.5 h; anodic oxidation: carbon-paste plate as anode, stainless-steel plate as cathode, constant current intensity of 1A, an anodic density of 63 mA/cm2; Further byproducts given;
参考文献
Barba, Isidoro; Tornero, Marcial
Tetrahedron, 1992 , vol. 48, # 45 p. 9967 - 9976
反应条件
sodium methylate
T=25 - 30°C; 1.5 h; anodic oxidation: carbon-paste plate as anode, stainless-steel plate as cathode, constant current intensity of 1A, an anodic density of 63 mA/cm2; Further byproducts given;
参考文献
Barba, Isidoro; Tornero, Marcial
Tetrahedron, 1992 , vol. 48, # 45 p. 9967 - 9976
反应条件
sodium methylate
T=25 - 30°C; 1.5 h; anodic oxidation: carbon-paste plate as anode, stainless-steel plate as cathode, constant current intensity of 1A, an anodic density of 63 mA/cm2; Further byproducts given;
参考文献
Barba, Isidoro; Tornero, Marcial
Tetrahedron, 1992 , vol. 48, # 45 p. 9967 - 9976
参考文献
Claisen
Chemische Berichte, 1898 , vol. 31, p. 1020
参考文献
Rose, Phillip D. R.; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 9 p. 1589 - 1595
