3,4-二乙酰氧基苯甲醛合成路线 （共 15 条）
反应条件
1.1: 1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
1.3: 20 °C
2.1: Pd(OPiv)2; [bis(acetoxy)iodo]benzene / α,α,α-trifluorotoluene / 120 °C / Inert atmosphere
2.2: 20 °C
3.1: pyridine
View Scheme
参考文献
Huang, Chunhui; Ghavtadze, Nugzar; Chattopadhyay, Buddhadeb; Gevorgyan, Vladimir
Journal of the American Chemical Society, 2011 , vol. 133, # 44 p. 17630 - 17633
反应条件
1: titanium tetrachloride / dichloromethane / 4 h / -20 - -10 °C / |Inert atmosphere
2: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 2 h / 20 °C
View Scheme
参考文献
Madrid, Alejandro; Espinoza, Luis; Catalan, Karen; Gonzalez, Cesar; Montenegro, Ivan; Mellado, Marco; Werner, Enrique; Cuellar, Mauricio; Villena, Joan
Journal of the Chilean Chemical Society, 2013 , vol. 58, # 3 p. 1814 - 1816
反应条件
peracetoxy-β-cyclodextrine; Chirazyme
参考文献
Divakar, Soundar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 5 p. 1119 - 1122
反应条件
sodium iodide in acetonitrile
15 h; Ambient temperature; Product distribution;
参考文献
Corda, Luciana; Fadda, Anna Maria; Maccioni, Antonio; Maccioni, Anna Maria; Podda, Gianni
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 311 - 314
反应条件
1H-imidazole; thiophenol in tetrahydrofuran
T=0 - 20°C;
参考文献
Fumeaux, Rene; Menozzi-Smarrito, Candice; Stalmach, Angelique; Munari, Caroline; Kraehenbuehl, Karin; Steiling, Heike; Crozier, Alan; Williamson, Gary; Barron, Denis
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 22 p. 5199 - 5211
