N-(4-氨基-3-吡啶基)-乙酰胺盐酸盐(1:1)合成路线 （共 4 条）
反应条件
in isobutyramide
T=22°C; 16 h;
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 - 25 °C / |Inert atmosphere
2: ethyl acetate / 16 h / |Inert atmosphere
3: hydrogenchloride / isopropyl alcohol
View Scheme
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 - 25 °C / |Inert atmosphere
2: ethyl acetate / 16 h / |Inert atmosphere
View Scheme
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=20 - 25°C; 16 h;
参考文献
Caron, Stephane; Do, Nga M.; McDermott, Ruth E.; Bahmanyar
Organic Process Research and Development, 2006 , vol. 10, # 2 p. 257 - 261
