2-硝基-4’-氯二苯硫醚合成路线 (共 10 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 9 h;
参考文献
Bandna; Guha, Nitul Ranjan; Shil, Arun K.; Sharma, Dharminder; Das, Pralay
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5318 - 5322
反应条件
potassium phosphate; copper(l) iodide; 2,9-dimethyl-1,10-phenanthroline in butan-1-ol T=120°C; 2 h; Microwave irradiation;
参考文献
Tan, Chen-Ming; Chen, Grace Shiahuy; Chena, Chien-Shu; Chern, Ji-Wang
Journal of the Chinese Chemical Society, 2011 , vol. 58, # 1 p. 94 - 100
反应条件
potassium carbonate in ethanol; water
参考文献
The University of Connecticut
Patent: US5679695 A1, 1997 ;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 46, # 12 p. 3814 - 3817
参考文献
Hidaka, Hiroyoshi
Patent: US6403607 B1, 2002 ;
反应条件
isopropyl-benzene; triethyl phosphite Heating;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2437 - 2441
参考文献
The University of Connecticut
Patent: US5679695 A1, 1997 ;
反应条件
dihydrogen peroxide; acetic acid
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1749 - 1757
反应条件
1: aq. H2O2, AcOH
2: Fe, aq. HCl
3: (i) (diazotization), (ii) NaN3
View Scheme
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 1749 - 1757