1: With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 1 h; 2: With chloro-trimethyl-silane in tetrahydrofuran T=-78 - 20°C; 1 h; 3: With hydrogenchloride more than 3 stages;
参考文献
TORAY INDUSTRIES, INC.
Patent: EP2009006 A1, 2008 ;
Location in patent: Page/Page column 110 ;