1: via (R)-(+)-α-methylbenzylamine salt
2: SOCl2; DMF / CHCl3 / 1 h / 60 °C
3: 441 mg / pyridine / CH2Cl2 / 0.5 h
View Scheme
参考文献
Shan, Guomin; Stoutamire, Donald W.; Wengatz, Ingrid; Gee, Shirley J.; Hammock, Bruce D.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 5 p. 2145 - 2155
1: SOCl2; DMF / CHCl3 / 1 h / 60 °C
2: 441 mg / pyridine / CH2Cl2 / 0.5 h
View Scheme
参考文献
Shan, Guomin; Stoutamire, Donald W.; Wengatz, Ingrid; Gee, Shirley J.; Hammock, Bruce D.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 5 p. 2145 - 2155
1: HCl / tetrahydrofuran; H2O / 0.5 h / 20 °C
2: 441 mg / pyridine / CH2Cl2 / 0.5 h
View Scheme
参考文献
Shan, Guomin; Stoutamire, Donald W.; Wengatz, Ingrid; Gee, Shirley J.; Hammock, Bruce D.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 5 p. 2145 - 2155
Shan, Guomin; Stoutamire, Donald W.; Wengatz, Ingrid; Gee, Shirley J.; Hammock, Bruce D.
Journal of Agricultural and Food Chemistry, 1999 , vol. 47, # 5 p. 2145 - 2155