2,3-二氢-1,4-苯并二恶烷-6-羰酰氯合成路线 (共 4 条)
反应条件
thionyl chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 18 h;
参考文献
TRAGEX PHARMA; HADJ-SLIMANE, Reda; GARBAY, Christiane
Patent: WO2012/156289 A1, 2012 ;
Location in patent: Page/Page column 31 ;
反应条件
1: KMnO4 2: SOCl2 View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 1 p. 71 - 85
反应条件
1: acetyl chloride; aluminium chloride; carbon disulfide 2: alkaline aqueous sodium hypochlorite solution 3: thionyl chloride View Scheme
反应条件
1: alkaline aqueous sodium hypochlorite solution 2: thionyl chloride View Scheme