1: benzene / 1.5 h
2: 96 percent / dinitrogen trioxide / dimethylformamide / 2 h / 0 °C
3: 55 percent Spectr. / 1 N sodium hydroxide / ethanol / 0.08 h / Ambient temperature
View Scheme
参考文献
Miyahara; Kamiya; Nakadate
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 1 p. 41 - 44
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反应条件
in acetonitrile
added p-toluidine to a soln. of Ru-complex; stirred for 30 min at room temp.; evapd. to dryness; extracted with ice-cold water; filtrated; added β-naphthol with stirring over a period of 15 min; sepd.; recrystd. from methanol; dried residue obtained after water extraction; dissolved in CH2Cl2; added hexane; filtered; dried in vacuo; elem. anal.;
参考文献
Deb, Alok Kumar; Goswami, Sreebrata
Polyhedron, 1991 , vol. 10, p. 1799 - 1802
