2,3-二溴苯并-1,4-二噁烷合成路线 （共 6 条）
反应条件
sodium iodide in acetone 2 h; Heating / reflux;
参考文献
Coudert, Gerard; Ayerbe, Nathalie; Lepiere, Franck; Routier, Sylvain; Caignard, Daniel-Henri; Renard, Pierre; Hickman, John; Pierre, Alain; Leonce, Stephane
Patent: US2006/40930 A1, 2006 ;
Location in patent: Page/Page column 9 ;
参考文献
Moureu
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1899 , vol. 128, p. 559
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 295
Full Text Show Details
Moureu
Annales de Chimie (Cachan, France), 1899 , vol. <7> 18, p. 130
反应条件
sodium iodide in acetone Heating; Yield given;
参考文献
Dorrestijn, Edwin; Epema, Onno J.; Van Scheppingen, Wibo B.; Mulder, Peter
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 5 p. 1173 - 1178
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
Irradiation;
参考文献
Dorrestijn, Edwin; Epema, Onno J.; Van Scheppingen, Wibo B.; Mulder, Peter
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 5 p. 1173 - 1178
反应条件
1: 83 percent / t-BuOK / diethyl ether / 8 h / 20 °C
2: 75 percent / NiCl2(dppp) / diethyl ether / 2 h / 20 °C
View Scheme
参考文献
Lee, Thomas V.; Leigh, Alistair J.; Chapleo, Christopher B.
Tetrahedron, 1990 , vol. 46, # 3 p. 921 - 934
参考文献
Moureu
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1899 , vol. 128, p. 559
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 295
Full Text Show Details
Moureu
Annales de Chimie (Cachan, France), 1899 , vol. <7> 18, p. 130
