1,5-二氢-3-甲氧基-2,4-苯并二氧杂环庚合成路线 (共 3 条)
反应条件
toluene-4-sulfonic acid in ethylene glycol dimethyl ether T=20°C; 1 h;
参考文献
Journal of Organometallic Chemistry, , vol. 656, # 1-2 p. 168 - 176
反应条件
toluene-4-sulfonic acid in ethylene glycol dimethyl ether
0.5 h; Ambient temperature;
参考文献
Machinaga, Nobuo; Kibayashi, Chihiro
Tetrahedron Letters, 1989 , vol. 30, # 31 p. 4165 - 4168
反应条件
1: LiAlH4 / diethyl ether / Ambient temperature
2: 86 percent / p-toluenesulfonic acid / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature
View Scheme
参考文献
Machinaga, Nobuo; Kibayashi, Chihiro
Tetrahedron Letters, 1989 , vol. 30, # 31 p. 4165 - 4168