(Z)-5-癸烯-1-醇乙酸酯合成路线 （共 44 条）
反应条件
pyridine in hexane T=12 - 20°C; Acetylation; 2 h;
参考文献
Bykov; Butenko; Egupova; Finkelshtein
Russian Chemical Bulletin, 2000 , vol. 49, # 7 p. 1301 - 1304
参考文献
Tortajada, Amparo; Mestres, Ramon; Iglesias-Arteaga, Martin A.
Synthetic Communications, 2003 , vol. 33, # 10 p. 1809 - 1814
反应条件
hydrogen; nickel; ethylenediamine in ethanol T=20°C;
参考文献
Chobanyan
Russian Journal of Applied Chemistry, 2004 , vol. 77, # 12 p. 2036 - 2037
反应条件
1: n-pentyltriphenylphosphonium bromide With sodium hydride in tetrahydrofuran; dimethyl sulfoxide T=10 - 25°C; 2: 5-oxopent-1-yl acetate in tetrahydrofuran; dimethyl sulfoxide Wittig reaction; 24 h;
参考文献
Tortajada, Amparo; Mestres, Ramon; Iglesias-Arteaga, Martin A.
Synthetic Communications, 2003 , vol. 33, # 10 p. 1809 - 1814
参考文献
US2010/113837 A1, ;
Page/Page column 5 ;
反应条件
1: 68.4 percent / MoCl5/SiO2; SnMe4 / toluene / 24 h / 20 °C / 19000 Torr 2: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 2 h 3: 9-BBN; OH(1-) 4: Py View Scheme
参考文献
Tetrahedron, , vol. 55, # 27 p. 8249 - 8252
反应条件
1: diisobutylaluminum hydride / diethyl ether; toluene / 1.5 h / -10 °C 2: 91 percent / pyridine / 24 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 1.1 p. 46 - 49
Zhurnal Organicheskoi Khimii, , vol. 26, # 1 p. 57 - 61
反应条件
1.1: Cp2ZrHCl; HCl 2.1: 9-BBN; OH- 2.2: pyridine View Scheme
参考文献
Doklady Chemistry, , vol. 384, # 4-6 p. 163 - 166
反应条件
1: 55 g / Me4Sn / MoCl5/SiO2 / toluene / 24 h / 20 °C 2: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 1 h / 20 °C 3: 92 percent / 9-BBN; NaOH; H2O2 / tetrahydrofuran; methanol 4: 93 percent / pyridine / hexane / 2 h / 12 - 20 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 49, # 7 p. 1301 - 1304
反应条件
1: 92 percent / cation-exchange resin KU-2-8 H(1+) form / methanol / 5 h / Ambient temperature 2: H2 / Ni-P2 3: pyridine View Scheme
参考文献
Chemistry of Natural Compounds, , vol. 24, # 1 p. 130 - 131
Khimiya Prirodnykh Soedinenii, , vol. 24, # 1 p. 143 - 145
