2,6-二甲基-4-氧代-2-环己烯-1-羧酸甲酯合成路线 （共 5 条）
反应条件
lithium chloride in water; dimethyl sulfoxide T=145°C; 6 h; Inert atmosphere;
参考文献
Majetich, George; Allen, Scott
Arkivoc, 2010 , vol. 2010, # 4 p. 104 - 124
反应条件
piperidine in ethanol
T=-5 - 100°C; Inert atmosphere;
参考文献
Majetich, George; Allen, Scott
Arkivoc, 2010 , vol. 2010, # 4 p. 104 - 124
反应条件
piperidine in methanol
T=20°C; 48 h;
参考文献
Kim, Sung Hwan; Lee, Hyun Seung; Park, Bo Ram; Kim, Jae Nyoung
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1725 - 1728
反应条件
sodium hydride
1.) THF, RT, 30 min, 2.) THF, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Wada, Eiji; Funakoshi, Junji; Kanemasa, Shuji
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 9 p. 2456 - 2464
反应条件
oxygen; copper diacetate; trifluoroacetic acid; lithium bromide in acetonitrile
T=80°C; P=760.051 Torr; 10 h; Sealed tube;
参考文献
Tong, Hung-Chun; Reddy, K. Rajender; Liu, Shiuh-Tzung
European Journal of Organic Chemistry, 2014 , vol. 2014, # 15 p. 3256 - 3261
