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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
673-41-6
合成路线
（共 139 条）
673-41-6
+
78-94-4
丁烯酮
→
反应条件
3506-75-0
4-(4-氯苯基)-2-丁酮
反应条件
titanium(III) chloride in acetic acid T=5°C; other α,β-unsaturated carbonyl compounds, regioselectivity of aryl radical addition; Product distributionRate constantMechanism;
参考文献
Citterio, Attilio; Minisci, Francesco; Vismara, Elena
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 81 - 88
75-30-9
2-碘代丙烷
+
673-41-6
+
78-94-4
丁烯酮
→
反应条件
637-87-6
对氯碘苯
+
3506-75-0
4-(4-氯苯基)-2-丁酮
+
110-12-3
5-甲基-2-己酮
反应条件
titanium(III) chloride in acetic acid T=5°C; 2 h; var. conc. of reagents; Product distributionRate constant;
参考文献
Citterio, Attilio; Minisci, Francesco; Vismara, Elena
Journal of Organic Chemistry, 1982 , vol. 47, # 1 p. 81 - 88
673-41-6
+
81290-20-2
(三氟甲基)三甲基硅烷
→
反应条件
407-16-9
对氯三氟甲基苯硫醚
反应条件
1: 1-(4-chlorophenyl)diazonium tetrafluoroborate With copper(I) isothiocyanate; sodium isothiocyanate; caesium carbonate in acetonitrile T=20°C; 0.166667 h; Inert atmosphere; 2: (trifluoromethyl)-trimethylsilane in acetonitrile T=20°C; 16 h;
参考文献
Danoun, Gregory; Bayarmagnai, Bilguun; Gruenberg, Matthias F.; Goossen, Lukas J.
Chemical Science, 2014 , vol. 5, # 4 p. 1312 - 1316
108-22-5
乙酸异丙烯酯
+
673-41-6
→
反应条件
5586-88-9
4-氯苯基丙酮
反应条件
potassium acetate in water; acetone T=20°C;
参考文献
Molinaro, Carmela; Mowat, Jeffrey; Gosselin, Francis; O'Shea, Paul D.; Marcoux, Jean-Francois; Angelaud, Remy; Davies, Ian W.
Journal of Organic Chemistry, 2007 , vol. 72, # 5 p. 1856 - 1858
108-31-6
马来酸酐
+
673-41-6
→
反应条件
3152-15-6
3-(4-氯苯基)-2,5-呋喃二酮
反应条件
[(t-Bu)2P(OH)]2PdCl2 ; sodium acetate in acetonitrile Heck Reaction; 1 h; Reflux;
参考文献
Canto, Karen; Da Silva Ribeiro, Rodrigo; Biajoli, Andre F. P.; Correia, Carlos Roque D.
European Journal of Organic Chemistry, 2013 , # 35 p. 8004 - 8013
111-34-2
乙烯基正丁醚
+
673-41-6
→
反应条件
2050-68-2
+
4251-65-4
+
99-91-2
反应条件
1: With [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate in acetonitrile T=30°C; Heck reaction; 0.5 h; 2: With hydrogenchloride in water; acetonitrile T=25°C; 0.5 h;
参考文献
Machado, Angelo H.L.; de Sousa, Marcio A.; Patto, Daniela C.S.; Azevedo, Luiz F.S.; Bombonato, Fernanda I.; Correia, Carlos Roque D.
Tetrahedron Letters, 2009 , vol. 50, # 11 p. 1222 - 1225
673-41-6
+
106-51-4
→
反应条件
15232-10-7
+
33685-58-4
+
1988-11-0
+
20307-43-1
反应条件
2-iodo-propane; copper in dimethyl sulfoxide 3 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
673-41-6
+
123-31-9
→
反应条件
20307-43-1
+
108-90-7
+
106-51-4
反应条件
phosphate buffer; water in acetonitrile T=25°C; var. pH; Rate constantMechanism;
参考文献
Brown, Kathlynn C.; Doyle, Michael P.
Journal of Organic Chemistry, 1988 , vol. 53, # 14 p. 3255 - 3261
75-30-9
2-碘代丙烷
+
673-41-6
+
106-51-4
→
反应条件
637-87-6
对氯碘苯
+
15232-10-7
+
33685-58-4
+
1988-11-0
+
20307-43-1
反应条件
copper in dimethyl sulfoxide T=20°C; 1 h; other catalyst, other time; Rate constantMechanismProduct distribution;
参考文献
Citterio, Attilio; Vismara, Elena; Bernardi, Rosanna
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 876 - 890
673-41-6
→
反应条件
20307-43-1
+
75877-78-0
反应条件
in water; acetonitrile Rate constant;
参考文献
Becker, H. G. O.; Jirkovsky, J.; Fojtik, A.; Kleinschmidt, J.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 505 - 511
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