4-甲氧基苯基-1,3-二噻戊环合成路线 （共 30 条）
反应条件
1: 86 percent / kaolinitic clay / Heating
2: 76 percent / Heating; kaolinitic clay
View Scheme
参考文献
Jnaneshwara; Barhate; Sudalai; Deshpande; Wakharkar; Gajare; Shingare; Sukumar
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 965 - 968
参考文献
Fasbender
Chemische Berichte, 1888 , vol. 21, p. 1475
Chemische Berichte, 1887 , vol. 20, p. 461
反应条件
1: sodium iodide; p-benozquinone / acetonitrile; water / 24 h / 100 °C
2: copper(II) sulfate / dichloromethane / 20 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
1: With copper(l) iodide in chloroform
T=20°C; 0.166667 h;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform
1 h;
3: With water in chloroform
T=20°C; 12 h;
参考文献
Fu, Liang; Yao, Chang-Jiang; Chang, Ning-Jie; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 506 - 508
反应条件
1.1: sodium iodide; p-benozquinone / acetonitrile; water / 24 h / 100 °C
2.1: copper(II) sulfate / dichloromethane / 20 °C
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -20 °C
3.2: -20 - 0 °C
4.1: sodium iodide; p-benozquinone / acetonitrile; water / 19 h / 100 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Yamada, Tetsuya; Kato, Sei-Ichi; Kikkawa, Shoko; Kondo, Yoshinori
Tetrahedron, 2013 , vol. 69, # 44 p. 9192 - 9199
反应条件
1: triphenylmethyl perchlorate
2: Na
View Scheme
参考文献
Okuyama, Tadashi; Fujiwara, Wataru; Fueno, Takayuki
Journal of the American Chemical Society, 1984 , vol. 106, # 3 p. 657 - 662
反应条件
triphenylmethyl perchlorate
参考文献
Okuyama, Tadashi; Fujiwara, Wataru; Fueno, Takayuki
Journal of the American Chemical Society, 1984 , vol. 106, # 3 p. 657 - 662
反应条件
1: With copper(l) iodide in chloroform
T=20°C; 0.166667 h;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform
1 h;
3: With water in chloroform
T=20°C; 12 h;
参考文献
Fu, Liang; Yao, Chang-Jiang; Chang, Ning-Jie; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 506 - 508
反应条件
bromine in tetrachloromethane
0.833333 h; Ambient temperature;
参考文献
Caputo, Romualdo; Ferreri, Carla; Palumbo, Giovanni; Capozzi, Giuseppe
Tetrahedron, 1986 , vol. 42, # 8 p. 2369 - 2376
反应条件
1: With copper(l) iodide in chloroform
T=20°C; 0.166667 h;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform
1 h;
3: With water in chloroform
T=20°C; 12 h;
参考文献
Fu, Liang; Yao, Chang-Jiang; Chang, Ning-Jie; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 506 - 508
