1-苯基-2-丁炔-1-酮合成路线 （共 27 条）
反应条件
1: 92 percent / Na2SO4; pyridine / methanol / 20 °C 2: 99 percent / ICl / CH2Cl2 / 0.75 h / 20 °C View Scheme
参考文献
Waldo, Jesse P.; Larock, Richard C.
Organic Letters, 2005 , vol. 7, # 23 p. 5203 - 5205
反应条件
triethylamine in diethyl ether
参考文献
Renzi,G. et al.
Gazzetta Chimica Italiana, 1968 , vol. 98, p. 656 - 666
反应条件
copper(l) iodide; triethylamine in N,N-dimethyl acetamide T=80°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 67, # 1 p. 95 - 98
反应条件
triethylamine in diethyl ether
参考文献
Renzi,G. et al.
Gazzetta Chimica Italiana, 1968 , vol. 98, p. 656 - 666
反应条件
manganese(IV) oxide; acetone
参考文献
Bharucha
Journal of the Chemical Society, 1956 , p. 2446
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=30°C; 0.5 h;
参考文献
Verkruijsse, H. D.; Heus-Kloos, Y. A.; Brandsma, I.
Journal of Organometallic Chemistry, 1988 , vol. 338, p. 289 - 294
反应条件
anhydrous iron chloride in nitromethane
T=-15°C; 6 h; Inert atmosphereSeal tube;
参考文献
Gandeepan, Parthasarathy; Parthasarathy, Kanniyappan; Su, Tsu-Hui; Cheng, Chien-Hong
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 457 - 468
反应条件
in tetrahydrofuran; diethyl ether
T=-20 - 20°C;
参考文献
Xu, Bao-Hua; Kehr, Gerald; Froehlich, Roland; Wibbeling, Birgit; Schirmer, Birgitta; Grimme, Stefan; Erker, Gerhard
Angewandte Chemie - International Edition, 2011 , vol. 50, # 31 p. 7183 - 7186
反应条件
lt;Ph3P(1+)gt;2O*2OTf(1-); triethylamine in 1,2-dichloro-ethane
1 h; Heating;
参考文献
Hendrickson, James B.; Hussoin, Md. Sajjat
Synthesis, 1989 , # 3 p. 217 - 218
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; 4 h;
参考文献
Cox, Christopher D.; Breslin, Michael J.; Mariano, Brenda J.
Tetrahedron Letters, 2004 , vol. 45, # 7 p. 1489 - 1493
