2,6-二甲基庚-1,5-二烯合成路线 （共 12 条）
参考文献
Henne; Chanan
Journal of the American Chemical Society, 1944 , vol. 66, p. 393
反应条件
bei der Ozonspaltung;
参考文献
Henne; Chanan
Journal of the American Chemical Society, 1944 , vol. 66, p. 393
参考文献
Auwers; Moosbrugger
Justus Liebigs Annalen der Chemie, 1912 , vol. 387, p. 179
反应条件
1: CH2Cl2 / 0 °C 2: Et3N / CH2Cl2 3: KO-t-Bu / tetrahydrofuran; 2-methyl-propan-2-ol View Scheme
参考文献
Block,E.; Aslam,M.; Eswarakrishnan,V.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4568
反应条件
potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=-23 - 25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Block, Eric; Eswarakrishnan, Venkatachalam; Gebreyes, Kassu
Tetrahedron Letters, 1984 , vol. 25, # 48 p. 5469 - 5472
反应条件
1: CH2Cl2 / 0 °C 2: Et3N / CH2Cl2 3: KO-t-Bu / tetrahydrofuran; 2-methyl-propan-2-ol View Scheme
参考文献
Block,E.; Aslam,M.; Eswarakrishnan,V.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4568
反应条件
potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=-23 - 25°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Block, Eric; Eswarakrishnan, Venkatachalam; Gebreyes, Kassu
Tetrahedron Letters, 1984 , vol. 25, # 48 p. 5469 - 5472
反应条件
1: 25 percent / tetraphenylporphine, O2 / CH2Cl2 / 4 h / -50 °C
2: triphenylphosphine
View Scheme
参考文献
Uchida, Minoru; Nakagawa, Kazuyuki; Negishi, Tsutomu; Asano, Shoji; Mori, Kenji
Agricultural and Biological Chemistry, 1981 , vol. 45, # 2 p. 369 - 372
参考文献
Wallach; Scheunert
Justus Liebigs Annalen der Chemie, 1902 , vol. 324, p. 102
Chem. Zentralbl., 1902 , vol. 73, # I p. 1295
参考文献
Tiemann
Chemische Berichte, 1900 , vol. 33, p. 3707
