7-氧杂二环[4.1.0]庚烷-2-酮合成路线 （共 57 条）
反应条件
1,1,1-trifluoro-N,N-bis(2-methoxyethyl)silanamine in dichloromethane T=0 - 20°C;
参考文献
MERCK and CO., INC.; KATZ, Jason; KNOWLES, Sandra, L.; JEWELL, James, P.; SLOMAN, David, L.; STANTON, Matthew, G.; NOUCTI, Njamkou
Patent: WO2010/17046 A1, 2010 ;
Location in patent: Page/Page column 44; 51 ;
WO 2010/017046 A1
反应条件
tetrakis(triphenylphosphine) palladium(0); 1,2-bis-(diphenylphosphino)ethane in water; toluene T=80°C; 24 h;
参考文献
Suzuki, M.; Watanabe, A.; Noyori, R.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2095 - 2096
反应条件
Amberlyst 15; sodium iodide in acetone T=20°C; deoxygenation; 3 h;
参考文献
Tetrahedron, , vol. 56, # 12 p. 1733 - 1737
反应条件
dirhodium tetraacetate in benzene 0.75 h; Heating;
参考文献
Tetrahedron Letters, , vol. 25, # 3 p. 251 - 254
参考文献
House; Wasson
Journal of the American Chemical Society, 1957 , vol. 79, p. 1488,1490
反应条件
pyridine; 2,4-dinitrobenzenesulfonhydrazide in tetrahydrofuran
参考文献
Corey,E.J.; Sachdev,H.S.
Journal of Organic Chemistry, 1975 , vol. 40, # 5 p. 579 - 581
反应条件
palladium diacetate; ethylene glycol; N-ethyl-N,N-diisopropylamine; poly(ethylene glycol) in water; acetonitrile T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
jones' reagent 1) acetone, 15-20 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Krishna, R. R.; Chawla, H. P. S.; Dev, Sukh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1190 - 1196
参考文献
House; Wasson
Journal of the American Chemical Society, 1957 , vol. 79, p. 1488,1490
反应条件
trichlorophosphate RT, 30 min, heating, 4-4.5 h;
参考文献
Tetrahedron Letters, , vol. 36, # 32 p. 5819 - 5822
