1: 92 percent / toluene-p-sulphonic acid / toluene / 18 h / Heating
2: 87 percent / LiAlH4 / diethyl ether / 3 h / Ambient temperature
3: 74 percent / CrO3, 3,5-dimethylpyrazole / CH2Cl2 / 1.25 h / -30 °C
4: 88 percent / ethylenediamine / nitromethane / 4 h / Heating
View Scheme
参考文献
Parkinson, Christopher J.; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1053 - 1057
1: 87 percent / LiAlH4 / diethyl ether / 3 h / Ambient temperature
2: 74 percent / CrO3, 3,5-dimethylpyrazole / CH2Cl2 / 1.25 h / -30 °C
3: 88 percent / ethylenediamine / nitromethane / 4 h / Heating
View Scheme
参考文献
Parkinson, Christopher J.; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1053 - 1057
