反应条件
1: 1.) BH3*SMe2, 2.) aq. NaOH, H2O2 / 1.) 0 deg C - RT, 1.5 h, 2.) a) ) deg C, 30 min, b) 50 deg C, 1 h 2: 98 percent / pyridine / 1 h / 0 °C 3: 84 percent / LDA / 1.) -78 deg C, 30 min, 2.) RT, 30 min 5: 5percent sodium amalgam / tetrahydrofuran; methanol / 9 h / -20 - 20 °C 6: n-Bu4NF / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 26 p. 5311 - 5320
