2,4,6-三氯-5-氟嘧啶合成路线 (共 5 条)
反应条件
N,N-dimethyl-aniline; trichlorophosphate T=110°C; 24 h;
参考文献
WO2011/50200 A1, ;
Page/Page column 90 ;
WO 2011/050200 A1
反应条件
hydrogenchloride T=160°C; P=22501.8 Torr; 4 h;
参考文献
Journal of Fluorine Chemistry, , vol. 45, p. 417 - 430
反应条件
hydrogenchloride T=200°C; P=75006 Torr; 3 h;
参考文献
Baasner, B.; Klauke, E.
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 417 - 430
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethyl acetate T=50°C; P=3000.2 Torr;
参考文献
Baasner, B.; Klauke, E.
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 417 - 430
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethyl acetate T=30°C; P=2625.2 Torr;
参考文献
Baasner, B.; Klauke, E.
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 417 - 430