1,1,4,4,6-五甲基-1,2,3,4-四氢化萘合成路线 （共 36 条）
反应条件
aluminium trichloride 12 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 56, # 15 p. 4706 - 4713
反应条件
1: 2,5-dimethyl-2,5-dihydroxy hexane With hydrogenchloride in water T=20°C; 1 h; 2: toluene With AlCl3, aluminium chloride in dichloromethane T=20°C; 3 h;
参考文献
US2005/148590 A1, ;
Page/Page column 14; 15 ;
反应条件
AlCl3, aluminium chloride in toluene 0.416667 h;
参考文献
EP1105120 B1, ;
Page/Page column 13 ;
EP 1105120 B1
反应条件
hydrogenchloride; AlCl3 in toluene
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 1 h;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 36, # 7 p. 701 - 712
反应条件
1: HCl conc. / 3 h / 20 °C 2: 99 percent / AlCl3 / CH2Cl2 / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 17 p. 5772 - 5782
反应条件
1: 87 percent / LiAlH4 / diethyl ether / 1 h / Heating 2: 79 percent / POCl3, pyridine / 100 °C 3: 80 percent / H2 / 10percent Pd/C / ethyl acetate / 1 h View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 36, # 7 p. 701 - 712
反应条件
1: 79 percent / POCl3, pyridine / 100 °C 2: 80 percent / H2 / 10percent Pd/C / ethyl acetate / 1 h View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 36, # 7 p. 701 - 712
反应条件
Wilkinson's catalyst in toluene Heating;
参考文献
Helvetica Chimica Acta, , vol. 72, p. 1537 - 1553
反应条件
1: 1.) NBS, 2.) 1-methylpyrrolidin-2-one, 3.) PCC / 1.) CCl4, 77 deg C, 45 min, 2.) H2O, 100 h, 1h, 3.) CH2Cl2, 20 deg C, 2 h 2: <RhCl(PPh3)3> / toluene / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 72, p. 1537 - 1553
