lithium aluminium tetrahydride in tetrahydrofuran Heating;

hydrogen; cobalt T=150 - 170°C; P=183877 Torr; Hydrierung des Reaktionsprodukts an Kupfer-Zinkoxid bei 250grad/250 at;

hydrogen; cobalt T=150 - 170°C; P=183877 Torr; Hydrierung des Reaktionsprodukts an Kupfer-Zinkoxid bei 250grad/250 at;

1: 96 percent / p-toluenesulfonic acid / 1 h / Heating 2: 92 percent / Jones reagent / acetone 3: oxalyl chloride / 0.5 h / Ambient temperature 4: N-hydroxypyridine-2-thione sodium salt, 4-dimethylaminopyridine, bromotrichloromethane / CCl4 / 0.25 h / Heating 5: 73 percent / lithium aluminium hydride / tetrahydrofuran / Heating View Scheme

1: 92 percent / Jones reagent / acetone 2: oxalyl chloride / 0.5 h / Ambient temperature 3: N-hydroxypyridine-2-thione sodium salt, 4-dimethylaminopyridine, bromotrichloromethane / CCl4 / 0.25 h / Heating 4: 73 percent / lithium aluminium hydride / tetrahydrofuran / Heating View Scheme

1: oxalyl chloride / 0.5 h / Ambient temperature 2: N-hydroxypyridine-2-thione sodium salt, 4-dimethylaminopyridine, bromotrichloromethane / CCl4 / 0.25 h / Heating 3: 73 percent / lithium aluminium hydride / tetrahydrofuran / Heating View Scheme

1: N-hydroxypyridine-2-thione sodium salt, 4-dimethylaminopyridine, bromotrichloromethane / CCl4 / 0.25 h / Heating 2: 73 percent / lithium aluminium hydride / tetrahydrofuran / Heating View Scheme

2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride T=80°C; 0.666667 h; varying Bu3SnH concentrations; Product distributionRate constant;

2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride T=80°C; 0.666667 h; varying Bu3SnH concentrations; Product distributionRate constant;