反应条件
diphenyldisulfane in benzene
byproducts: (PhS)2Hg; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSSPh (2.0 equiv) in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 2.5h);; filtration; solvent removed (vacuum); PhS(CH2)6SPh analysed by (1)H NMR, GLC and GCMS;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538