1,8-二氮杂双环[5.4.0]十一碳-7-烯合成路线 （共 79 条）
反应条件
tri(n-propyl)amine; sodium methylate in methanol
参考文献
General Electric Company
Patent: US2004/59151 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
1: oxalyl bromide / 1,2-dichloro-ethane / 7 h / 0 - 25 °C 2: anisole; MeOH / 1,2-dichloro-ethane / 0.5 h / 25 °C 3: amberlite IRA 400 (OH(-)) / methanol View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 4 p. 478 - 482
反应条件
1.1: NaH / tetrahydrofuran / 0.5 h / 20 °C 1.2: tetrabutylammonium iodide / tetrahydrofuran / 20 °C 2.1: oxalyl bromide / 1,2-dichloro-ethane / 7 h / 0 - 25 °C 3.1: anisole; MeOH / 1,2-dichloro-ethane / 0.5 h / 25 °C 4.1: amberlite IRA 400 (OH(-)) / methanol View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 4 p. 478 - 482
反应条件
in chloroform-d1 T=19.84°C; 56 h;
参考文献
Carafa, Marianna; Iannone, Francesco; Mele, Valentina; Quaranta, Eugenio
Green Chemistry, 2012 , vol. 14, # 12 p. 3377 - 3385
反应条件
in chloroform-d1 T=19.84°C; 16 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 13 p. 2458 - 2465
反应条件
T=150°C; 2 h; Product distribution;
参考文献
Matsumura, Noburu; Nishiguchi, Hiroshi; Okada, Masao; Yoneda, Shigeo
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 3 p. 885 - 887
反应条件
T=180°C; 2 h; Product distribution;
参考文献
Matsumura, Noburu; Nishiguchi, Hiroshi; Okada, Masao; Yoneda, Shigeo
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 3 p. 885 - 887
反应条件
T=180°C; 2 h; Product distribution;
参考文献
Matsumura, Noburu; Nishiguchi, Hiroshi; Okada, Masao; Yoneda, Shigeo
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 3 p. 885 - 887
参考文献
Green Chemistry, , vol. 14, # 12 p. 3377 - 3385
反应条件
in acetonitrile Equilibrium constant; Solvent;
参考文献
Inorganic Chemistry, , vol. 52, # 9 p. 5273 - 5283
