2,3,3-三氟丙烯酰氟合成路线 （共 13 条）
反应条件
α,α,α-trifluorotoluene; titanium tetrachloride; Titanium(IV) oxide
T=130°C; P=9000.7 Torr; 20 h;
参考文献
Schwertfeger, W.; Siegemund, G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 237 - 246
反应条件
SbF5 in neat (no solvent)
参考文献
England, David C.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 4007 - 4008
反应条件
ClSO2F (sulfuryl chloride fluoride); SbF5
参考文献
Chepik, S. D.; Belen'kii, G. G.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 8.2 p. 1712 - 1714
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 8 p. 1926 - 1928
反应条件
oxygen; mercury; Nitrous oxide
Irradiation; Further byproducts given;
参考文献
Stockburger,L.; Heicklen,J.
Journal of the American Chemical Society, 1971 , vol. 93, p. 3331 - 3336
参考文献
Cheburkov,Yu.A.; Bargamova,M.D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 801 - 806
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 833 - 840
反应条件
nitrogen(II) oxide; mercury
Irradiation;
参考文献
Tarrant,P.; Savory,J.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1728 - 1730
参考文献
Knunyants,I.L. et al.
Tetrahedron, 1973 , vol. 29, p. 595 - 601
参考文献
Murotani, Eisuke; Saito, Susumu; Sawaguchi, Masanori; Yamamoto, Hiromasa; Nakajima, Youji; Miyajima, Tatsuya; Okazoe, Takashi
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1131 - 1136
反应条件
sodium hydrogencarbonate
1) 48 h, steam bath, 2) H2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
England, David C.; Donald, Elaine A.; Weigert, Frank J.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 144 - 147
反应条件
48 h; Heating; Title compound not separated from byproducts;
参考文献
England, David C.; Donald, Elaine A.; Weigert, Frank J.
Journal of Organic Chemistry, 1981 , vol. 46, # 1 p. 144 - 147
