2-(三氟甲基)-1H-咪唑合成路线 （共 7 条）
反应条件
para-dicyanobenzene; tetraethylammonium tetrafluoroborate in N,N-dimethyl-formamide
electrolysis; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Medebielle, Maurice; Pinson, Jean; Saveant, Jean-Michel
Journal of the American Chemical Society, 1991 , vol. 113, # 18 p. 6872 - 6879
反应条件
sulfur(IV) fluoride; hydrogen fluoride
T=70°C; 48 h;
参考文献
Owen, D.; Plevey, R. G.; Tatlow, J. C.
Journal of Fluorine Chemistry, 1981 , vol. 17, p. 179 - 186
反应条件
tetraethylammonium tetrafluoroborate; para-dicyanobenzene in N,N-dimethyl-formamide
(indirect electrochemical reduction of the perfluoroalkyl halide in the presence of imidazolate anion); Yield given. Yields of byproduct given;
参考文献
Medebielle, Maurice; Pinson, Jean; Saveant, Jean-Michel
Tetrahedron Letters, 1990 , vol. 31, # 9 p. 1279 - 1282
反应条件
in methanol
168 h; Ambient temperatureIrradiation;
参考文献
Kimoto, Hiroshi; Fujii, Shozo; Cohen, Louis A.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2867 - 2872
反应条件
in N,N-dimethyl-formamide
10 h; Irradiation;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 645 - 648
反应条件
in methanol
168 h; Ambient temperatureIrradiationvar. perfluoroalkyl iodides; other imidazoles; Product distributionMechanism;
参考文献
Kimoto, Hiroshi; Fujii, Shozo; Cohen, Louis A.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2867 - 2872
反应条件
in diethyl ether
T=18°C; 24 h; Yield given;
参考文献
Owen, D.; Plevey, R. G.; Tatlow, J. C.
Journal of Fluorine Chemistry, 1981 , vol. 17, p. 179 - 186
