5-羟基-2-甲氧基黄酮合成路线 （共 12 条）
反应条件
acetic acid in water
T=110°C; 24 h;
参考文献
Kralj, Ana; Nguyen, Mai-Thao; Tschammer, Nuska; Ocampo, Nicolette; Gesiotto, Quinto; Heinrich, Markus R.; Phanstiel, Otto
Journal of Medicinal Chemistry, 2013 , vol. 56, # 12 p. 5019 - 5032
反应条件
1: potassium carbonate; potassium iodide / acetone / |Reflux; |Inert atmosphere
2: potassium hydroxide / methanol / 19 h / 85 °C
3: iodine / dimethyl sulfoxide / 140 °C
4: acetic acid / water / 24 h / 110 °C
View Scheme
参考文献
Kralj, Ana; Nguyen, Mai-Thao; Tschammer, Nuska; Ocampo, Nicolette; Gesiotto, Quinto; Heinrich, Markus R.; Phanstiel, Otto
Journal of Medicinal Chemistry, 2013 , vol. 56, # 12 p. 5019 - 5032
反应条件
1: potassium hydroxide / methanol / 19 h / 85 °C
2: iodine / dimethyl sulfoxide / 140 °C
3: acetic acid / water / 24 h / 110 °C
View Scheme
参考文献
Kralj, Ana; Nguyen, Mai-Thao; Tschammer, Nuska; Ocampo, Nicolette; Gesiotto, Quinto; Heinrich, Markus R.; Phanstiel, Otto
Journal of Medicinal Chemistry, 2013 , vol. 56, # 12 p. 5019 - 5032
反应条件
1: iodine / dimethyl sulfoxide / 140 °C
2: acetic acid / water / 24 h / 110 °C
View Scheme
参考文献
Kralj, Ana; Nguyen, Mai-Thao; Tschammer, Nuska; Ocampo, Nicolette; Gesiotto, Quinto; Heinrich, Markus R.; Phanstiel, Otto
Journal of Medicinal Chemistry, 2013 , vol. 56, # 12 p. 5019 - 5032
反应条件
1: potassium hydroxide / methanol / 19 h / 85 °C
2: iodine / dimethyl sulfoxide / 140 °C
3: acetic acid / water / 24 h / 110 °C
View Scheme
参考文献
Kralj, Ana; Nguyen, Mai-Thao; Tschammer, Nuska; Ocampo, Nicolette; Gesiotto, Quinto; Heinrich, Markus R.; Phanstiel, Otto
Journal of Medicinal Chemistry, 2013 , vol. 56, # 12 p. 5019 - 5032
反应条件
1: NaNH2
2: acetic acid; aqueous hydrochloric acid
3: aqueous hydriodic acid; phenol / 160 °C
4: acetone; potassium carbonate
View Scheme
参考文献
Gallagher et al.
Journal of the Chemical Society, 1953 , p. 3770,3777
反应条件
1: aqueous hydriodic acid; phenol / 160 °C
2: acetone; potassium carbonate
View Scheme
参考文献
Gallagher et al.
Journal of the Chemical Society, 1953 , p. 3770,3777
反应条件
1: aluminium chloride; benzene
2: acetone; potassium carbonate
View Scheme
参考文献
Gallagher et al.
Journal of the Chemical Society, 1953 , p. 3770,3777
反应条件
1: NaNH2
2: acetic acid; aqueous hydrochloric acid
3: aqueous hydriodic acid; phenol / 160 °C
4: acetone; potassium carbonate
View Scheme
参考文献
Gallagher et al.
Journal of the Chemical Society, 1953 , p. 3770,3777
反应条件
1: acetic acid; aqueous hydrochloric acid
2: aluminium chloride; benzene
3: acetone; potassium carbonate
View Scheme
参考文献
Gallagher et al.
Journal of the Chemical Society, 1953 , p. 3770,3777
