乙基(2-甲氧基苯基)(氧代)乙酸酯合成路线 （共 14 条）
反应条件
boric acid; [Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=60°C; 3 h;
参考文献
Shimizu, Hiroshi; Murakami, Masahiro
Chemical Communications, 2007 , # 27 p. 2855 - 2857
反应条件
1: 2-methoxybromobenzene With n-butyllithium in diethyl ether; pentane T=-70°C; 0.75 h; 2: oxalic acid diethyl ester in diethyl ether; pentane T=-70 - 20°C; 1 h;
参考文献
US2004/180878 A1, ;
Page/Page column 20 ;
反应条件
n-butyllithium in tetrahydrofuran T=-78°C;
参考文献
Chiu; Jordan
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5763 - 5766
参考文献
BEECHAM GROUP PLC
Patent: EP386940 A1, 1990 ;
反应条件
in diethyl ether T=-78°C; 1 h; Inert atmosphere;
参考文献
Infante, Rebeca; Nieto, Javier; Andres, Celia
Chemistry - A European Journal, 2012 , vol. 18, # 14 p. 4375 - 4379
反应条件
chromium(VI) oxide; sulfuric acid
参考文献
Journal of Organic Chemistry, , vol. 73, # 10 p. 3842 - 3847
反应条件
aluminium trichloride in chloroform T=0 - 5°C; 1.33333 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 3 p. 810 - 814
反应条件
aluminium trichloride in dichloromethane T=0 - 5°C; 1.33333 h; modification without solvent (other time); Title compound not separated from byproducts;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 57, # 3 p. 810 - 814
反应条件
n-butyllithium 1.) ether, RT, 26 h, 2.) 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 20, # 12 p. 1781 - 1791
